Organic Syntheses, Volume 96

Discussion Addendum for: 4-Nonylbenzoic Acid 1
Alois Fuerstner

Late-Stage Deoxyfluorination of Phenols with PhenoFluorMix 16
Junting Chen and Tobias Ritter

Nickel-Catalyzed Cross-Coupling of 2-Methoxynaphthalene with Methyl 4-(5,5-dimethyl-1,3,2-dioxaborinan-2-yl)benzoate 36
Yuki Kawashima, Takayuki Furukawa, Naoto Chatani and Mamoru Tobisu

Discussion Addendum for: Lithium Amides as Homochiral Ammonia Equivalents for Conjugate Additions to ?,?-Unsaturated Esters: Asymmetric Synthesis of (S)-?-Leucine 53
Stephen G. Davies, Ai M. Fletcher, Paul M. Roberts, and James E. Thomson

Synthesis of 2,3-Diaryl-2H-azirines via Cs2CO3-Mediated Cyclization of Ketoxime Acetates 66
Mi-Na Zhao and Zheng-Hui Guan

Discussion Addendum for: The Direct Acyl-Alkylation of Arynes. Preparation of Methyl 2- (2-acetylphenyl)acetate 80
Austin C. Wright and Brian M. Stoltz

Discussion Addendum for: Convenient Preparation of 3-Ethoxycarbonyl Benzofurans from Salicylaldehydes and Ethyl Diazoacetate 98
Mizzanoor Rahaman and M. Mahmun Hossain

Discussion Addendum for: Phosphine-Catalyzed [4 + 2] Annulation: Synthesis of Ethyl 6-Phenyl-1-tosyl-1,2,5,6-tetrahydropyridine-3-carboxylate 110
Aslam C. Shaikh and Ohyun Kwon

Discussion Addendum for: Protection of Alcohols using 2-Benzyloxy-1-methylpyridinium Trifluoromethanesulfonate: Methyl (R)-(-)-3-Benzyloxy-2-methyl Propanoate 124
Harvey F. Fulo, Philip A. Albiniak, and Gregory B. Dudley

Synthesis of 4-Methylbenzoate(2',4',6'-trimethoxy-phenyl)iodonium Tosylate 137
Thomas L. Seidl, Aaron Moment, Charles Orella, Thomas Vickery, and David R. Stuart

Gold-Catalyzed Oxidative Coupling of Arenes and Arylsilanes 150
Chris Nottingham, Verity Barber, and Guy C. Lloyd-Jones

Discussion Addendum for: Preparation of Enantioenriched Homoallylic Primary Amines 179
Miguel Yus

Discussion Addendum for: Synthesis of Ynamides by Copper-Mediated Coupling of 1,1-Dibromo-1-alkenes with Nitrogen Nucleophiles. Preparation of 4-Methyl-N-(2-phenylethynyl)-N-(phenylmethyl)benzenesulfonamide 195
Cedric Theunissen, Pierre Thilmany, Mounsef Lahboubi, Nicolas Blanchard, and Gwilherm Evano

Discussion Addendum for: Phosphine-Catalyzed [3 + 2] Annulation: Synthesis of Ethyl 5-(tert-Butyl)-2-phenyl-1-tosyl-3-pyrroline-3-carboxylate 214
Aslam C. Shaikh and Ohuyn Kwon

Discussion Addendum for: Synthesis of Highly Enantiomerically Enriched Amines by Asymmetric Transfer Hydrogenation of N-(tert-Butylsulfinyl) Imines 232
Miguel Yus

Synthesis of Chiral Diamine Ligands for Nickel-catalyzed Asymmetric Cross-couplings of Alkylchloroboronate Esters with Alkylzincs: 1R,2R)-N,N'-Dimethyl-1,2-bis(2-methylphenyl)-1,2-diaminoethane 245
Yusuke Masuda and Gregory C. Fu

Preparation of 5-(Triisopropylalkynyl) dibenzo[b,d] thiophenium triflate 258
Bernd Waldecker, Kevin Kafuta, and Manuel Alcarazo

Three-Step Synthesis of 2-(Diiodomethyl)-4,4,5,5-tetramethyl- 1,3,2-dioxaborolane from Dichloromethane 277
Morgane Sayes, Guillaume Benoit, and Andre B. Charette

Discussion Addendum for: Allylic Oxidation Catalyzed by Dirhodium(II) Tetrakis[?-caprolactamate] of tert-Butyldimethylsilylprotected trans-Dehydroandrosterone 300
Yong-Liang Su, Luca De Angelis and Michael P. Doyle

Preparation of (R)-3-(3,5-Bistrifluoromethylphenyl)-1,1'-bi-2-naphthol 312
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada

Catalytic Enantioselective Addition of an In-Situ Prepared Aryltitanium Reagent to p-Chloroacetophenone: (R)-(+)-1-(4-Chlorophenyl)-1-m-tolylethanol 333
Yusuke Kobayashi, Atsushi Matsuda, Tomoya Ushimaru, and Toshiro Harada

Stereoselective Synthesis of (R)-((R)-1-Phenyl-2,2,2-trichloroethyl)-2-(2-bromophenyl)aziridine-1-carboxylate 351
Helene Lebel and Henri Piras

Discussion Addendum for: Preparation of (R,R)-1,2:4,5-Diepoxypentane 361
Nicholas Sizemore and Scott D. Rychnovsky

(R)-N,N'-Dimethyl-1,1'-binaphthyldiamine 382
Scott E. Denmark and Pavel Ryabchuk

Preparation of a Diisopropylselenophosphoramide Catalyst and its Use in Enantioselective Sulfenoetherification 400
Scott E. Denmark, Pavel Ryabchuk, Hyung Min Chi, and Anastassia Matviitsuk

anti-1,2,2,3,4,4-Hexamethylphosphetane 1-Oxide 418
Trevor V. Nykaza, Julian C. Cooper, and Alexander T. Radosevich

Facile Reduction of Amides Using Nickel Catalysis: Reduction of 12-Aminododecanolactam 436
Bryan J. Simmons, Melissa Ramirez, and Neil K. Garg

Preparation of 2,4,5,6-Tetra(9H-carbazol-9-yl)isophthalonitrile 455
Saskia M. Engle, Takisha R. Kirkner, and Christopher B. Kelly

Discussion Addendum for: Fluorobis(phenylsulfonyl)methane (FBSM) 474
Xanath Ispizua-Rodriguez, Vinayak Krishnamurti, Mathew Coe, and G. K. Surya Prakash

Synthesis of 5-Hydroxy-4-methoxy-2-methylpyrylium Trifluoromethanesulfonate from Kojic Acid 494
Nana B. Agyemang and Ryan P. Murelli

Iridium-Catalyzed Reductive Coupling of Grignard Reagents and Tertiary Amides 511
Pablo Gabriel, Lan-Gui Xie, and Darren J. Dixon

Synthesis of Chiral Tetramic Acids: Preparation of (S)-5-Benzylpyrrolidine-2,4-dione from L-Phenylalanine Methyl Ester Hydrochloride 528
Kyle M. Lambert, Austin W. Medley, Amy C. Jackson, Lauren E. Markham, and John L. Wood

Synthesis of 8-Hydroxygeraniol 586
Francesca M. Ippoliti, Joyann S. Barber, and Neil K. Garg

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organic chemistry; synthesis; experimental procedures; synthetic methods; transformations; reagents; building blocks; intermediates; medicinal chemistry