Organic Syntheses, Volume 97

Discussion Addendum for: Synthesis of Arylboronic Pinacol Esters from Corresponding Arylamines 1
Fanyang Mo, Di Qiu, and Jianbo Wang

Deaminative Functionalization of Primary Sulfonamides 12
Patrick S. Fier and Kevin M. Maloney

Synthesis of 3,6-Bis(dimethylamino)-9H-xanthen-9-one by Stepwise Chemical Redox Cycling 21
James L. Bachman, Cyprian I. Pavlich, and Eric V.Anslyn

Preparation of (-)-Levoglucosenone from Cellulose Using Sulfuric Acid in Polyethylene Glycol 38
J. Klepp, W. Dillon, Y. Lin, P. Feng, and B. W. Greatrex

Scalable Preparation of O-(Diphenylphosphinyl) hydroxylamine (DPPH) 54
Tamas Benkovics, Andrew J. Neel, Ralph Zhao, and Gregory J. Hughes

Discussion Addendum for: Dibenzo[a,e]cyclooctene: Multigram Synthesis of a Bidentate Ligand 66
Guenter Helmchen

Discussion Addendum for: (S)-(-)-2-Allylcyclohexanone (2-Allylcyclohexan-1-one] 79
Manfred Braun

Synthesis of 4-Nitrophenyl (2,2,6,6-Tetramethylpiperidin-1-yl) Carbonate (NPTC) for N-Protection of L-Phenylalanine Ethyl Ester 96
Joseph R. Lizza and Peter Wipf

Discussion Addendum for: Pd-Catalyzed External-CO-Free Carbonylation: Preparation of 2,4,6-Trichlorophenyl 3,4-Dihydronaphthalene-2-Carboxylate 125
Hideyuki Konishi and Kei Manabe

From 5-Hydroxynicotinic Acid to Nitrogenous (4+3)-Cycloadducts 139
Alexander S. Harmata and Michael Harmata

Synthesis of ?-Bromoacetyl MIDA Boronate 157
C. Frank Lee, Chieh-Hung Tien, Shinya Adachi, and Andrei K. Yudin

Synthesis of Chiral Bisoxazoline Ligands: (3aR,3a'R,8aS,8a'S)-2,2'- (cyclopropane-1,1-diyl)bis(3a,8a-dihydro-8H-indeno[1,2-d]oxazole) 172
Julie L. Hofstra, Travis J. DeLano, and Sarah E. Reisman

Synthesis of 2,5-Diaryloxadiazinones 189
Andrew V. Kelleghan, Katie A. Spence, and Neil K. Garg

Preparation of O-Pivaloyl Hydroxylamine Triflic Acid 207
Szabolcs Makai, Eric Falk, and Bill Morandi

Preparation of a Z-Iodoalkene through Stork-Zhao-Wittig Olefination, Stereo-retentive Lithium-iodine Exchange and Z-Boronic acid Pinaco Ester Synthesis 217
Mathieu A. Morin, Samantha Rohe, Cecile Elgindy, and Michael S. Sherburn

Discussion Addendum for: Synthesis of Substituted Indazoles via [3 + 2] Cycloaddition of Benzyne and Diazo Compounds 232
Anton V. Dubrovskiy and Richard C. Larock

Anhydrous, Homogeneous, Suzuki-Miyaura Cross-Coupling of Boronic Esters using Potassium Trimethylsilanolate 245
Connor P. Delaney, Ethan M. Heyboer, and Scott E. Denmark

Stereoselective Synthesis of Chiral Sulfinamide Monophosphine Ligands (Ming-Phos)(S, Rs)-M 262
Anjing Hu, Zhan-Ming Zhang, Yuanjing Xiao, and Junliang Zhang

Preparation of Asymmetric Phase-transfer Catalyst, 1,4-Bis((4S,5S)- 1,3-bis(3,5-di-tert-butylbenzyl)-4,5-diphenylimidazolidin-2-ylidene)piperazine-1,4-diium chloride 274
Esther Cai Xia Ang, Xinyi Ye, and Choon-Hong Tan

Oxidation of Aldehydes to Nitriles with an Oxoammonium Salt: Preparation of Piperonylonitrile 294
Nathaniel D. Kaetzel, Kyle M. Lambert, and Christopher B. Kelly

Preparation of 1H-Indazole-3-carbonitrile 314
Yonggang Chen, Qinghao Chen, Lushi Tan, Lu Chen, and Xiaowei Wang

Asymmetric Michael Addition of Dimethyl Malonate to 2-Cyclopenten-1-one Catalyzed by a Heterobimetallic Complex 327
Nicholas J. Fastuca, Alice R. Wong, Victor W. Mak, and Sarah E. Reisman

Discussion Addendum for: Synthesis of Et2SBr*SbCl5Br and its Use in Biomimetic Brominative Polyene Cyclizations 339
Cooper A. Taylor and Scott A. Snyder

Nickel-Catalyzed Arylboration of Cyclopentene 355
Stephen R. Sardini and M. Kevin Brown

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• Química orgânica

organic chemistry; synthesis; experimental procedures; synthetic methods; transformations; reagents; building blocks; intermediates; medicinal chemistry